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Mass of crucible and hydrated compound: 16.08g
Mass of crucible and anhydrous compound(first heating): 14.55g
Mass of crucible and anhydrous compound(second heating): 14.55g
Observations:
The MgSO4•xH2O turned a more white color and seemed to melt into a single mass. It started off as clear granules(like table salt), and ended up as a single white mass. Mass went down after heating.
Analysis:
Mass of anhydrous compound: 14.55g-13.08g=1.47g MgSO4
Mass of water in hydrated compound: 3g-1.47g=1.53g H2O
Moles of anhydrous compound: 1.47g/(24.30+32.06+4*16.00)=12.2*10-3 mol MgSO4
Moles of water in hydrated compound: 1.53g/(2*1.008+16.00)=84.9*10-3 mol H2O
Ratio of moles of anhydrous compound to moles of water: 12.2*10-3/12.2*10-3 mol MgSO4:84.9*10-3/12.2*10-3 mol H2O=1:6.959 ~1:7 mol. MgSO4•7H2O.
Conclusion:
The purpose of this lab was to use hydrated compounds to practice calculating how many water molecules are attached to hydrated compounds. We achieved this purpose by heating and weighing hydrated compounds until there was no water left and calculating the difference between the hydrated compound and anhydrous compound to find how much water was in the hydrated compound. Potential sources of error may be inaccuracies in weighing, contamination, or water that didn't get evaporated. Potential improvements may include a moisture-free environment, and a better controlled heating colution and weighing system. From the analysis, there was about 1.53g of water in the 3g of MgSO4•xH2O, leaving about 1.47g of MgSO4, ~51% H2O.